The axial motion of the new Phoenix goniometer is ensured by the direct-drive
motors which are being controlled by encoders, allowing to achieve an angular
resolution of about 0.00001[deg] and a direct coupling between motors and load,
without any use of transmission device like straps or gears mostly affected by inertial
concerns, elasticity and frequent mechanical failures.
X-Ray Diffraction (XRD) provides any additional information beyond basic identification. If the sample
is a mixture, XRD data are to be analyzed to define the proportion of the different
phases contained.
Further information should include the degree of crystallinity of the phase(s)
contained and the deviations of the sample from their ideal composition.
Maximum rated output |
3 kW |
Rated tube voltage |
60 kV |
Rated tube current |
60 mA |
Control method |
Remote |
Stability |
< 0.1% |
Target |
Cr, Fe, Co, Cu, Mo, Ag, W |
Focus size |
Fine Focus (FF) 0.4 mm ! 8 mm Long Fine Focus (LFF) 0.4 mm ! 12 mm Normal Focus (NF) 1.0 mm ! 10 mm Broad Focus (BF) 2.0 mm ! 8 mm |
Tube shield |
One window with electromagnetic shutter |
Radiation enclosure |
Full safety shielding according to international guidelines |
Goniometer radius |
180 mm, 210 mm, 240 mm |
2-theta measurement range (at 210 mm radius) |
- 5 [deg] to 157 [deg] |
Slits |
set of Fixed slits |
Slewing speed |
1000 deg/min |
Scanning speed |
from 0.01 to 20 deg/min |
Step width |
0.0001 to 1 degree |
Automatic alignment |
for reflectometry, automatic positioning |
Monochromator |
flat or curved |
Counting linearity |
up to 1 MHz |
Scintillating counter |
from 5 to 100 keV, 10 MHz max. counts YAP(Ce) crystal |
Solid state detector |
Linear strip detector, CCD area |