PHOENIX TORQUE

X-Ray Diffractometer


A new driving force in X-Ray Diffraction


The specificity of the direct drive motors makes the new Phoenix goniometer unique in its gender, providing an extreme accuracy in positioning it and avoiding any use of additional mechanical device as well.

The axial motion of the new Phoenix goniometer is ensured by the direct-drive motors which are being controlled by encoders, allowing to achieve an angular resolution of about 0.00001[deg] and a direct coupling between motors and load, without any use of transmission device like straps or gears mostly affected by inertial concerns, elasticity and frequent mechanical failures.

Direct Drive Torque Motors
  • High efficiency
  • Low noise
  • Longer lifetime
  • High torque at low rpm
  • Faster and accurate positioning
  • Drive Stiffness


Highly reduced vibrations improve the precision of the goniometer motions; through the encoders the position of each motor can to be simultaneously controlled by means of a steady comparison between the command and the returned signals in order to immediately carry out any eventual readjustment.


Powder analysis


X-Ray Diffraction (XRD) provides any additional information beyond basic identification. If the sample is a mixture, XRD data are to be analyzed to define the proportion of the different phases contained. Further information should include the degree of crystallinity of the phase(s) contained and the deviations of the sample from their ideal composition.
  • Qualitative Phase identification
  • Peak position and structure determination
  • Phase quanti?cation
  • Phase transition
  • Crystallinity

THIN FILM ANALYSIS
The parallel beam geometry ensures the phase identification of thin films along with the determination and comparison of reflective profiles and film thickness. Enhanced optical device for collimation purposes provides high resolution rocking curve.
TRANSMISSION ANALYSIS
The advantageous modular configuration for XRD transmission analysis coupled with high speed detectors is oriented to high resolution phase identification.

SMALL ANGLE X-RAY SCATTERING
Through the use of a high speed solid state detector, SAXS measurements become extremely easy to perform.

X-Ray Diffraction (XRD)

Data sheet


HV X-Ray Generator and X-Ray Tube

 

Maximum rated output

3 kW

Rated tube voltage

60 kV

Rated tube current

60 mA

Control method

Remote

Stability

< 0.1%

Target

Cr, Fe, Co, Cu, Mo, Ag, W

Focus size

Fine Focus (FF) 0.4 mm ! 8 mm
Long Fine Focus (LFF) 0.4 mm ! 12 mm
Normal Focus (NF) 1.0 mm ! 10 mm
Broad Focus (BF) 2.0 mm ! 8 mm

Tube shield

One window with electromagnetic shutter

Radiation enclosure

Full safety shielding according to international guidelines

Goniometer radius

180 mm, 210 mm, 240 mm

2-theta measurement range (at 210 mm radius)

- 5 [deg] to 157 [deg]

Slits

set of Fixed slits



Goniometer

 

Slewing speed

1000 deg/min

Scanning speed

from 0.01 to 20 deg/min

Step width

0.0001 to 1 degree

Automatic alignment

for reflectometry, automatic positioning

Monochromator

flat or curved

Counting linearity

up to 1 MHz



Detector

 

Scintillating counter

from 5 to 100 keV, 10 MHz max. counts YAP(Ce) crystal

Solid state detector

Linear strip detector, CCD area

Documents


Brochure

PDF document

File size: 6.28 MByte

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